2 edition of quantitative separation of germanium and arsenic. found in the catalog.
quantitative separation of germanium and arsenic.
Harold J. Abrahams
Written in English
Thesis (PH. D.)--University of Pennsylvania, 1932.
|Statement||[by] Harold J. Abrahams.|
|LC Classifications||QD181.G5 A3 1932|
|The Physical Object|
|Number of Pages||10|
|LC Control Number||32016078|
The separation of germanium tetrachloride from arsenic trichloride by fractional distillation For reproduction of material from all other RSC journals and books: The separation of germanium tetrachloride from arsenic trichloride by fractional distillation. Determination of Silicon, Phosphorous, Arsenic, and Germanium as Heteropoly Acids Article in Journal of Analytical Chemistry 58(9) September with 34 Reads How we measure 'reads'.
Abstract. A method for the separation of carrier-free arsenic from bulk amount of germanium has been developed. 74,73 As has been produced through the reaction nat Ge(p,xn) 47,73 As with 13 MeV protons obtained from Variable Energy Cyclotron, Calcutta. The separation is performed by the distillation of Ge followed by anion exchange separation of As(V) using Dowex 1×8 anion exchange by: The results are presented of a study of the behaviour under uniaxial compression of absorption lines due to transitions from the ground state manifold of states of arsenic impurities in germanium to excited p states. It is found that the shear deformation potential constant Ell of the excited p states and conduction band minima of germanium is 164±02 eV. The equivalent deformation Cited by: 3.
Germanium (Ge) is considered a critical element due to its many industrial applications; Ge is a metalloid used in solar cells, fiber optics, metallurgy, chemotherapy, and polymerization catalysis. The main sources of Ge are sulfides ores of Zn, Pb, and Cu, coal deposits, as well as by-products and residues from the processing of these ores and coals (e.g., smelting flue dust and coal fly ashes).Cited by: 3. Unfortunately, this book can't be printed from the OpenBook. If you need to print pages from this book, we recommend downloading it as a PDF. Visit to get more information about this book, to buy it in print, or to download it as a free PDF. Below is the uncorrected machine-read text.
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From solutions with less than 7 N HCI germanium is practically not extracted by ligroin, while from the solutions with a higher concentration of hydrochloric acid Separation of germanium from arsenic it is readily extracted, the extraction being per cent.
at 10 N HC1, as seen from the data obtained t~or extraction with ligroin only (curve b in Fig. 1).Cited by: The Altmetric Attention Score is a quantitative measure of the attention that a research article quantitative separation of germanium and arsenic.
book received online. Clicking on the donut icon will load a page at with additional details about the score and the social media presence for the given by: 3.
Anion-Exchange Separation of Germanium from Arsenic(III and V) and Other Elements in Hydrochloric Acid-Acetic Acid Medium Quantitative Analysis of the Twenty Natural Protein Amino Acids by Gas-Liquid Chromatography.
Charles W. Gehrke & David L. Stalling. Editorial board page for “Separation Science”, Volume 2, Number 1. Determination of Germanium. Colorimetric Determination of Microgram Amounts with Oxidized Hematoxylin. Analytical Chemistry23 (7), DOI: /aca George Kingsley, Roscoe Schaffert, and W.
Harris. Microdetermination of Arsenic and Its Application to Biological by: Separation of germanium and arsenic from solutions by flotation. International Journal of Mineral Processing21 (), DOI: /(87)X.
Eric Heinen De Carlo, Christina Ronay. Separation off Silica from Spent Geothermal Fluids by Adsorptive Bubble by: Quantitative evaluation of germanium displacement induced by arsenic implantation using germanium isotope superlattices Article in Journal of End-to-End-testing () December.
The separation of arsenic from germanium was based on their relative affinities for different chromatographic materials in aqueous and organic environments. A quantitative micro-method for the separation of inorganic arsenite from arsenate in blood and urine T.
Crawford and I. Storey Departments of Medical Chemistry and Pharmacology, University of Cited by: 5. This book is composed of 43 chapters that also present sample preparation, separation, and precipitation protocols.
The first six chapters include Group I cations, such as silver, lead, mercury, copper, bismuth, and cadmium, followed by chapters on Group II cations, including arsenic, antimony, tin, germanium, gold, platinum, selenium, and Book Edition: 1.
About Germanium Arsenide. Germanium Arsenide is a crystalline solid used as a semiconductor and in photo optic applications.
American Elements produces to many standard grades when applicable, including Mil Spec (military grade); ACS, Reagent and Technical Grade; Food, Agricultural and Pharmaceutical Grade; Optical Grade. A simple, rapid, accurate, and reliable method of simultaneous determination of arsenic, germanium, phospohrus, and silicon is reported.
The method involves first, the determination of germanium as the phenylfluorone complex and its selective extraction with isoamyl by: 4. Arsenic and selenium speciation using HPLC–ICP–MS.
ICP–MS has revolutionised quantitative analysis of arsenic and selenium in rice grain. Efficient ionisation in the plasma results in high sensitivity enabling analysis even at the trace (μg L –1) levels found in uncontaminated rice grain, and the multi-element capability of the ICP–MS facilitates the identification of relationships Cited by: Separation of molybdoheteropoly acids of phosphorus, arsenic, silicon and germanium as ion-associates by HPLC.
Application to quantitative determination in water. Summary. Very low concentrations of Si(IV), Ge(IV), As(V) and P(V) in natural waters are determined by by: Crawford TB, Storey ID.
A quantitative micro-method for the separation of inorganic arsenite from arsenate in blood and urine. Biochem J. ; 38 (2)– [PMC free article] Graham AF, Crawford TB, Marrian GF. The action of arsine on blood: Observations on the nature of the fixed arsenic. Biochem J.
; 40 (2)–Cited by: 1. For example, Kraak and Walz [Kra65] reported electrophoretic separation of americium and curium from a solution containing M EDTA in a 4-h run, while Bächmann [Bäc66] has reported separation of actinium, americium, and curium from one another, as well as separation of various mixtures of actinides and lanthanides.
A summary of electrophoretic radiochemical procedures is available in the. Analytical Chemistry provides information pertinent to the fundamental aspects of analytical chemistry. This book discusses the development and methods in the field of air and water pollution control monitoring.
Organized into 14 chapters, this book begins with an overview of the quantitative and qualitative analysis for other analytical problems. Rapid and quantitative release, separation and determination of inorganic arsenic [As(III)+As(V)] in seafood products by microwave-assisted distillation and Cited by: Continuous gas-phase procedures for the separation of germanium and arsenic from fission products have been developed by Zendel and coworkers [Zen81].
The experimental arrangement they used is shown in Fig. A rapid and reliable method is also reported for the simultaneous determination of arsenic and silicon by selective extraction of silicomolybdic acid with isooctyl alcohol at pH.
A precise, simple and rapid method is described for the determination of inorganic arsenic [As(III)+As(V)] in seafood products.
The inorganic species were isolated from the matrix by microwave-assisted distillation and determined by hydride generation atomic absorption spectrometry (HGAAS). The microwave and chemic. Besides arsenic, small amount of selenium accompanied with germanium in hydrochloric acid distillation.
Presence of less than γ/50 ml. of it had little effect on the determination of.arsenic and molybdenum (7). Compound columns have been used for separation of uranium and thorium in ores (8,9). The uranium is eluted in ml, with a l/K nitric acid-ether eluent, and the thorium is eluted with a 12,5^ nitric acid-ether eluent.
Keaber (10) demonstrated a similar separation on a cellulose column. Cellulose columns with ether.Quantitative analysis with HPLC-ICPMS under gradient elution conditions with increasing content of organic solvents is severely restricted because the elemental response can vary significantly with the amount of carbon reaching the plasma.
The present work offers a solution to this challenge to elemental species quantification by introducing a volatile organic solvent directly into the spray.